wwPDB validation report of PDB entry 1DU2

The structure was determined by double and triple resonance heteronuclear NMR spectroscopy techniques. There is evidence of substantial conformational exchange in sections of the chain that severely limit the precision of the structure in these regions of the molecule. Specifically, conformational exchange occurs in the regions D19-M33 and L55-S63.

The structures are based on 819 restraints, 511 are NOE-derived distance constraints, 300 dihedral angle restraints and 8 distance restraints from hydrogen bonds

SOLUTION STRUCTURE OF THE THETA SUBUNIT OF DNA POLYMERASE III

geometric validation package for ligand chemistry in protein x-ray structures

assessment of nmr assigned chemical shifts

geometric validation of nmr ensemble structure

20191225.v01 (using entries in the PDB archive December 25th 2019)

domain identification of nmr ensemble structure

classification of nmr ensemble structure

nmr chemical shift validation and reference correction

random coil index prediction from nmr chemical shifts